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Fluid Inc. USGS-design Fluid Inclusion Microthermometric System

What it does: Fluid inclusion microthermometry is used to determine the crystallization temperatures of the minerals that contain them, and the salinity of fluids that were present in the formational setting during the time of crystallization.

Instrument Statistics: The Fluid Inc. fluid inclusion system uses a USGS-designed gas-heated and gas-cooled insulated stage. Observations for fluid inclusion work are performed using a Leica LaborluxS microscope and Hitachi HVD25 digital imaging system.
How it works: Small, mm-scale chips of crystalline minerals are mounted between thin glass plates in an area of the stage that contains a sensitive thermocouple and is surrounded by insulating material. Fluid inclusions, which are tiny bits of fluid trapped during crystal growth, are observed through the glass plates in the stage using a high-powered microscope. Samples are chilled or heated by passing heated or chilled gas, usually nitrogen, over them.

Crystals that grow in fluid-rich environments often trap a bit of the surrounding fluid in small inclusions within the grain. As the mineral cools, the liquid in the inclusion shrinks in volume and a vapor bubble appears. By heating the sample on a fluid inclusion stage until the bubble is reabsorbed, the "homogenization temperature" of the fluid inclusion is found. This temperature represents the minimum temperature at which the inclusion was trapped and therefore can be used to estimate the minimum temperature of mineral crystallization.

Freezing and melting temperatures can be determined by chilling fluid inclusions. Because the freezing and melting temperatures of the fluid are controlled by its salt content, the composition of fluids in the inclusion that were involved in crystal growth can be constrained.

Last updated 11/10

Observation area of fluid inclusion stage


Fluid inclusion containing fluid, a gas bubble, and salt crystals